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92.
Wenwen Xia Guodong Xia Guangsheng Tu Xin Dong Sumei Wang Rui Liu 《Ceramics International》2018,44(8):9125-9131
High-k oxide dielectric films have attracted intense interest for thin-film transistors (TFTs). However, high-quality oxide dielectrics were traditionally prepared by vacuum routes. Here, amorphous high-k alumina (Al2O3) thin films were prepared by the simple sol-gel spin-coating and post-annealing process. The microstructure and dielectric properties of Al2O3 dielectric films were systematically investigated. All the Al2O3 thin films annealed at 300–600?°C are in amorphous state with ultrasmooth surface (RMS ~ 0.2?nm) and high transparency (above 95%) in the visible range. The leakage current of Al2O3 films gradually decreases with the increase of annealing temperature. Al2O3 thin films annealed at 600?°C showed the low leakage current density down to 3.9?×?10?7 A/cm2 at 3?MV/cm. With the increase of annealing temperature, the capacitance first decreases then increases to 101.1?nF/cm2 (at 600?°C). The obtained k values of Al2O3 films are up to 8.2. The achieved dielectric properties of Al2O3 thin films are highly comparable with that by vapor and solution methods. Moreover, the fully solution-processed InZnO TFTs with Al2O3 dielectric layer exhibit high mobility of 7.23?cm2 V?1 s?1 at the low operating voltage of 3?V, which is much superior to that on SiO2 dielectrics with mobility of 1.22?cm2/V?1 s?1 at the operating voltage of 40?V. These results demonstrate that solution-processed Al2O3 thin films are promising for low-power and high-performance oxide devices. 相似文献
93.
Supercapacitors are a kind of novel energy storage devices with long cycle stability and high power density. Electrode materials selection is one of the key factors that affect the properties of supercapacitors. Biomass-derived electrode materials – being low cost, renewable and environmentally friendly – are therefore attracting researchers’ attention. In this work, we adopted a simple process of carbonization and activation with rice plant soot, a common biomass material, as carbon source, and finally obtained the nanoscale porous carbon electrode (NPCE) materials. Then, the electrochemical properties of the as-prepared NPCE materials were tested in 6 M KOH, and the results indicated that the specific capacitance could reach 216?Fg?1. Therefore, this low-cost, highly efficient technique is a significant milepost towards environmentally sustainable and commercially feasible fabrication of carbon electrode materials from biomass sources. 相似文献
94.
Zhao-Hua Mo Rui Yang Song Hong Yi-Xian Wu 《International Journal of Hydrogen Energy》2018,43(3):1790-1804
Introducing graphene into polymer matrix is an effective way to enhance performances of anion exchange membrane (AEM). However, utilizing the advantages of graphene by physical approach is limited due to the weak interface interaction between graphene and polymer matrix. Herein, we report an effective strategy to covalently bond graphene with polymer matrix to improve the interface interaction and further to improve the properties of AEM. A series of cross-linked quaternized graphene-based hybrid AEM were fabricated by covalently bonding poly (vinylbenzyl chloride) grafted graphene (GN-g-PVBC) copolymer with chloromethyl functionalized poly (styrene-b-isobutylene-b-styrene) (SIBS) through the cross-linker (N,N,N′,N′-tetramethyl-1,6-hexanediamine) by in-situ synthetic approach. The interface interaction between graphene and QSIBS is greatly enhanced according to micromorphology characterization of the hybrid membrane. The cross-linked quaternized hybrid AEM containing 0.55 wt% of GN-g-PVBC exhibits obviously improved dynamical mechanical properties (storage modulus: 418 MPa), ion conductivity (1.81 × 102 S cm?1), methanol barrier property (5.19 × 10?7 cm2 s?1), selectivity (3.49 × 104 S s cm?3) at 60 °C and especially a comparably excellent chemical stability to that of Nafion 115 due to the enhanced interface interaction between graphene and the polymer matrix. 相似文献
95.
很多熟料库在设计时未注意清库门的设置,或者是设计的清库门不合理从而给施工和后期的实际使用造成很多麻烦。本文介绍了几种熟料清库门的几种设计方案,对比了其设计方式,设计要点及优缺点,为熟料库设计提供了有益的思路。 相似文献
96.
我厂共有3台CRM4622型立式磨机生产矿渣粉,分别为#3,#4,#5立磨。其中#3,#4立磨(#3立磨投产于2010年,#4立磨投产于2012年)于2014年4月相继出现磨盘刮料架整体脱落情况。经过更换螺栓,情况得到暂时缓解。一段时间后,刮料架再次脱落。为了彻底解决刮料架脱落问题,决定对刮料架的固定方式进行改进,以提高刮料架的稳定性。 相似文献
97.
98.
100.
Guihua Liu Dan Luo Rui Gao Yongfeng Hu Aiping Yu Zhongwei Chen 《Small (Weinheim an der Bergstrasse, Germany)》2020,16(37)
The practical application of lithium–sulfur (Li–S) batteries is hindered by the “shuttle” of lithium polysulfides (LiPS) and sluggish Li–S kinetics issues. Herein, a synergistic strategy combining mesoporous architecture design and defect engineering is proposed to synthesize multifunctional defective 3D ordered mesoporous cobalt sulfide (3DOM N‐Co9S8?x) to address the shuttling and sluggish reaction kinetics of polysulfide in Li–S batteries. The unique 3DOM design provides abundant voids for sulfur storage and enlarged active interfaces that reduce electron/ion diffusion pathways. Meanwhile, X‐ray absorption spectroscopy shows that the surface defect engineering tunes the CoS4 tetrahedra to CoS6 octahedra on Co9S8, endowing abundance of S vacancies on the Co9S8 octahedral sites. The ever‐increasing S vacancies over the course of electrochemical process further promotes the chemical trapping of LiPS and its conversion kinetics, rendering fast and durable Li–S chemistry. Benefiting from these features, the as‐developed 3DOM N‐Co9S8?x/S cathode delivers high areal capacity, superb rate capability, and excellent cyclic stability with ultralow capacity fading rate under raised sulfur loading and low electrolyte content. This design strategy promotes the development of practically viable Li–S batteries and sheds lights on the material engineering in related energy storage application. 相似文献